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Search Results for design-of-experiments

Article
Exploring the Potentials of Laser Induced Forward Transfer  and Laser Annealing Processes for Synthesis/Printing of Silver Nanofilms on Quartz Substrates using Nd:YAG and CO2 Laser Beams

Hanadi H. Altawil

Pages: 118-123

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Abstract

Laser annealing represents a powerful method for tailoring the properties of silver nanofilms on quartz substrates, offering advantages in terms of precision, scalability, and functionalization. Continued research efforts are expected to deepen our understanding and broaden the applications of this promising technology in diverse fields. In this work, laser annealing of silver nanofilms deposited on quartz substrates was performed and investigated. RF CO2 laser of variable power in the range 1–20 W with beam quality of 1.1 was used to anneal silver nanofilms. AFM analysis emphasized that nanocrystal sizes of 60 nm were obtained for silver nanofilms. Furthermore, the optimum absorbance peak occurred at about 449 nm for smaller film thickness. Thermal simulation and analysis of the annealing process were also conducted using COMSOL Multiphysics software. It was observed that optimal temperature of 729 K was achieved when 10 W laser power and 2 mm/s scanning speed were used to anneal 20 nm silver film thickness. Design of expert analysis was also used to better understand the laser annealing process of silver nanofilms since convolution of several process parameters affect the process output.

Article
Characterization and Fabrication of Ankle Foot Orthoses using Composite with Titanium Nanoparticles

N.J. Khalaf, Sabrine Ben Amor, Borhen Louhichi

Pages: 109-117

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Abstract

Orthoses and prostheses were Chosen and laminated based on their high Yield, ultimate stresses, bending stresses, and fatigue limit. Response Surface Methodology (RSM) was utilized to find the best values for two parameters reinforcement perlon fiber and percent of Titanium Nanoparticle coupled with the matrix resin during optimization. The response surface methodology combined the expertise of mathematicians and statisticians to construct and analyze experimental models. Using this method, we identified 13 different lamination samples comprising a wide range of perlon number and Ti nano Wt% in their Perlon layer composition. All lamination materials defined by RSM methods and produced by a vacuum system were subjected to a battery of tests, with fatigue tests performed on the ideal laminating material in contrast to laminations created in the first study (Tensile test, Bending test, and Fatigue tests according to the ASTM D638 and D790 respectively). In comparison to the other 12 laminations tested using Design Expert version 10.0.2, the lamination with ten perlon layers and 0.75 percent Ti nano proved to be the strongest overall in terms of Yield, ultimate, and bending loads. This study used composite materials and titanium nanoparticles to characterize and fabricate ankle foot orthoses. Strength in bending should amount to about 70 MPa, around 85 MPa in tensile tension. Two empirical quadratic equations for the models of peak bending strength and maximum tensile stress with 95% confidence were created using the response surface approach and analysis of variance within the design of experiments software.

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