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Go to Editorial ManagerIn the present study, magnesium-based composites reinforced with different volume fractions (3, 5, 10, and 15) vol.% of micro sized Al2O3 particulates were fabricated by powder metallurgy technique which involves mixed, compacted and sintered. Powders were mixed by ball milling (without balls) for 6 hours at rotation speed 60 rpm. Then powder was compacted at 550 MPa and sintered at 530?C for 2 hours. Microstructures of sintered composites have been investigated by scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDX) and X-ray diffraction (XRD) energy dispersive. SEM image of sinter samples exhibit good bonding between the magnesium matrix and the alumina. The microhardness and wear resistance of micro composites has been improved significantly compared to that of pure magnesium. Highest value of microhardness is 97 HV at the volume fraction of 10 vol.% Al2O3.
The toxicity of permanent implants is the main concern. The release of ions from the substrate leads to toxicity. Because of how the human body works biologically, the toxicity of corrosion compounds is a byproduct of wear and fretting debris. aimed to improve the corrosion resistance of a 316L stainless steel substrate. Bio ceramic Nano-hydroxyapatite (HA) was coated using the Electrophoretic Deposition (EPD) technique. Stainless steel has good mechanical properties and high compatibility, but it suffers from body fluid attack due to its chloride content, which can penetrate the passivation layer, resulting in the release of chromium and nickel ions. Tissues and organs are damaged by the ions and debris that are released. To address this problem, it was coated with bioceramic using the EPD method. Suspensions of various powders—hydroxyapatite, magnesium oxide, zinc oxide, and the composite—were prepared and coated by electrophoretic deposition. The coated samples were dried at room temperature to ensure a homogeneous coating structure. The zeta potential test for magnesium oxide and hydroxyapatite suspensions was positive, while zinc oxide and complex suspensions were negative. One of the important parameters for achieving electrolyte and implant balance is the open circuit potential (OCP). A substantial change towards a more noble direction (less negative) was seen in the OCP-coated (316 L) alloy, suggesting excellent thermodynamic stability. Tafel extrapolation analysis was used to obtain the corrosion potential (Ecorr) and corrosion current density (Icorr) values of composite-coated stainless steel 316L, which are generally derived from the polarization curve. The findings that are in line with the MgO, HA, and ZnO coatings show a significant decrease in corrosion current (Icorr), an increase in corrosion potential (Ecorr), and a decrease in corrosion rate from (4.386 × 10-¹ mm/y) Stainless Steel 316 L to (1.417 × 10-² mm/y) MgO Coated and (1.222 × 10-³ mm/y) (65%MgO+25%ZnO+10%HA coated).
Magnesium oxide nanoparticles were deposited by laser pyrolysis process. Three types of lasers were employed CW CO2, Q-switched Nd-YAG (short pulses) and long pulses Nd-YAG lasers. The size and density of nanoparticles vary with laser energy, power, pulse duration and the scanning speed of the laser. In this method, MgO nanoparticles were deposited by a laser beam on a quartz substrate from aqueous solution of magnesium nitrate. AFM images reveal formation of small nanoparticle size of 24.5 nm with surface roughness 6.97nm by Q-switched Nd-YAG laser (10 ns) when the energy was 1J. While for CO2 laser, the smallest size was 18.8 nm at 0.4mm/s scanning speed with surface roughness 5.21nm at the same scanning speed. Moreover, long Nd-YAG pulses laser produces relatively larger average size of 37.5nm at 0.8ms pulse duration. The absorption spectra from UV-Visible spectroscopy were also conducted. The best absorption intensity was obtained at a wavelength ranging between 420-430 nm for both lasers. Finally, Thermal analysis using COMSOL Multiphysics software for the deposition process reveals that maximum temperature about 440Kfor Q-Switched Nd-YAG laser at 1J laser energy. While for RF CO2 laser, the maximum temperature obtained at 0.4mm/s scanning speed is 850K.This work provides a good knowledge for the deposition of nanoparticles using laser beams.
The aim of the research was for evaluation the morphological and chemical alterations that result from the Nd:YAG laser treatment of dental enamels using optical microscopy (OM) with Energy dispersion X-ray spectroscopy (EDX), respectively. Two human enamel samples were obtained, the samples were exposed to the Nd: YAG laser irradiation. The micrographs obtained by optical microscopy demonstrated morphological changes. The concentrations of carbon (C), calcium (Ca), phosphorus (P), and oxygen (O) in crater sites and its environs were measured using EDX, as well as trace amounts of manganese, magnesium, and silicon. However, due to their low concentration, these trace elements were neglected. We obtained the maximum depth profile of carters on tooth enamel surface at 1200 µm with laser pulse of 532 nm with 500 mJ energy/pulse, while the minimum depth profile of carters at 200 µm with laser pulse of 1064 nm with 100 mJ energy/pulse. Dental tissue can be safely treated with a Nd: YAG laser with 200 mJ, 9 ns, and 1064 nm since this laser irradiation range did not induce any noticeable morphological changes. As a result, the Nd: YAG laser offers as an ideal option for clinical treatment.