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Go to Editorial ManagerThe effects of the repeated solution heat treatment on hardness, tensile strength and microstructure of aluminum were investigated. For this purpose, an alloy of AA6061-T6 was undergo to cyclic solution heat treatment process which is composed of repeated period (10 min) held at 520 °C for 1, 4, 8 and 12 cycles. The hardness was tested for five aging times (as quenching, one week, three weeks, one month and five months) to all cycles (1, 4, 8 and 12) firstly and it is found that the hardness of five months as aging time for all cycles has the best results (90Hv) as compared with others (as quenching, one week, three weeks, and one month), so it was adopted for all cycles to implement the tensile test and the microstructure. Hardness results were improved to Vickers hardness of (90Hv) with increasing of cycles up to 8 cycles then decreasing after that to (45Hv). Tensile results were showed an increment (34%) also for the same group of 8 cycles compared with (17%) and (9%) for 4 and 12 cycles, respectively. Microstructure is revealed that whenever cycles are increased, the precipitate phase in alloy is increased also, thus, it is improved the hardness and tensile strength.
The current study presents the plasma cutting process of 2 mm thickness of AISI 1020 carbon steel. The experiment conducted by taking into the account the effect of two process parameters, including cutting current of 15 and 20 A with cutting speed in range of 500 - 4000 mm/min, on the kerf formation, microstructure and microhardness.The results showed that at low cutting current of 15 A the melting occurred at the workpiece surface without cutting action. Increase the current to 20 A led to full penetration of the workpiece material at low and high cutting speed, with kerf width between 1.26 mm and 1.1 mm for cutting speed of 500 mm/ min and 4000 mm/ min, respectively. The plasma arc cutting speed has a high impact on the heat-affected zone HAZ and microstructure development with coarse grains at the HAZ at low cutting speed of 500 mm/min and constant current of 20A, increase the plasma cutting speed led to decreasing the grain size. The microstructure of the HAZ exhibited a presence of perlite and ferrite with some martensite structure. The highest microhardness of the HAZ of 220.8 HV was found in the sample processed at 20 A current and high cutting speed of 4000 mm/ min. However, the minimum microhardness of the HAZ of 156.7 HV was found in the sample processed at 20 A current and low cutting speed of 500 mm/ min.
This paper presents a comparison of using different techniques for stir spot welding of Aluminum 2024-T3, which are refill friction stir spot welding (RFSSW), edited (RFSSW-pin) and conventional friction stir spot welding (FSSW), depending on the obtained tensile shear strength property. Specimens were prepared from AA2024-T3 sheet for chemical analysis and mechanical tests. Workpieces were stir spot welded utilizing the above mentioned techniques at four rotational speeds (2000, 2500, 3000 and 4000 rpm) using tool pin diameters (5 and 7 mm) for conducting the tensile shear tests. The microhardness along the cross section of the welded specimens was conducted at the best conditions as well as the microstructure examination. The comparison results revealed that at the rotational speeds (2000 and 4000 rpm) in both cases of tool pin (5 and 7 mm), the ultimate tensile shear force was slightly higher than that for other speeds. However, the ultimate tensile shear force was found higher at 3000 rpm speed with a tool pin 7 mm. The microhardness results manifested a W-shape at the best conditions. Finally, the microstructure examination depicted the morphology of the main zones of the weld joint.
Al2O3 is a major reinforcement in aluminum-based composites, which have been developing rapidly in recent years. The aim of this paper is to investigate the effect of alumina phases and amounts on the physical properties of fabricated Al-Al2O3 composite. Alpha micro and gamma nano of alumina with particle size of 30µm and 20 nm respectively reinforced aluminum matrix of 45 µm. The percentage of reinforcement material were in the range of (5, 10 and 15wt.%) fabricated by powder metallurgy technique. Specimens dimensions were a disc specimens with 11mm diameter and 5 mm thickness. The green density was achieved under compaction pressure of 500MPa, and then sintered under pressure less sintering at 500ºC in a vacuumed tube furnace for two hours Physical properties of the composite samples have been studied such as relative density, sintered density, porosity, microstructure characteristics, particles distribution, agglomeration, grain sizes and granularity accumulation distribution. It has been noticed that at the micro alumina phase, its relative densities are decreased when there is an increase in amount of micro alumina addition, on the contrary in case of nano composites, where the relative density are increasing along with the increase in nano alumina addition. At micro and nano composites, the produced relative densities are less than the pure aluminum relative density. Agglomeration are increasing with the increase in amount of reinforcement, while its more obvious with nano composite. Grain size reduced with the increase in amount of alumina in micro and nano composites, while, the obtained average grain size diameter is less in nano composite than in micro composites. It is obvious from the results that the variation in physical properties and microstructure of Al-Al2O3 composite are depends on both of alumina phases (size) and percentages. At 15wt.% of nano alumina higher relative density and lower porosity will be obtained.
Specimens with the structure of a face-centered cubic were produced using several sets of printing conditions. An experimental testing is conducted to carefully evaluate the microstructural analysis and compressive strength of this structure. The results include the measurement of mechanical properties, such as the peak stress. Fused deposition modeling is employed for the additive manufacturing of experimental specimens made from shape memory polymer thermoplastic polyurethane (MM-3520). We take into account the impact of printing factors on lattice structures, such as layer thickness, printing temperature, and printing speed. Analyzing the microstructure of the printed specimens exhibits that the specimens with highest printing temperature, lowest printing speed and thinner printing layer have better layers adhesion and lower porosities. All the mechanical tests are performed on specimens with the same structure and at a relatively constant density. Among the tested printing parameters, using a layer height of 0.1 mm, a printing temperature of 230 °C, and a printing speed of 20 mm/s yields the highest strength in the specimens. However, specimens printed with a layer height of 0.2 mm, a printing temperature of 220 °C, and a printing speed of 30 mm/s also exhibit good strength, albeit slightly lower than the maximum values. Additionally, when using these specific settings (0.3 mm – 210 °C – 40 mm/s), the mechanical qualities are minimized, yet the stress-strain curves exhibit characteristics similar to elastomers.
The Electrodeposition process has been used to prepare Nickel-Tungsten alloys on low carbon steel substrate by using ammonical citrate bath. The influence of deposition condition by variation of current density (0.04-0.2 A/cm2) and solution temperature (60-70 °C), on the microstructure was studied. The optical microscope and the scanning electron microscopy (SEM) were used to study the morphology of the deposit while the energy dispersive spectroscopy (EDS) was used to approximate the composition, in addition to X-Ray diffraction examination. The results show that the current efficiency has the major influence on the tungsten content in the alloys due to the formation of ternary complex which reflected into the properties of the deposit._x000D_ Keywords:
Aluminum metal matrix composites are widely employed for improving the mechanical properties. Various fabrication routes like liquid state, solid state and liquid-solid state are currently available for producing these materials. The objective of the present work is the fabrication of nano particulate composites AA7075-Al2O3 with different amount of nano particles (20-30 nm) reinforced material Al2O3 (2, 4 and 6 wt%) using stir casting technique at three stirring speeds (300, 850 and 1500 rpm). Tensile tests of these composites were carried-out to obtain the mechanical properties (ultimate strength and ductility). Vickers hardness tests were also performed to obtain the hardness number (VHN) of these materials. All tests were performed at room temperature. The microstructures of the best mechanical properties’ composites were examined for the three stirring speeds. It was revealed that the ultimate strength (?u) and Vickers hardness (VHN) for the composite containing 6 wt% Al2O3 fabricated at 850 rpm show the best properties compared to the other composites fabricated at 300 and 1500 rpm and the matrix. The ?u and VHN were increased by about (36.6 %) and (24.5 %) respectively. Ductility of the strongest composite (6 wt% Al2O3 at 850 rpm speed), however, was the least when compared to other composites and the matrix. With increasing the amount of Al2O3, ?u and VHN, an increasing trend was noticed while the ductility shows a reduction trend. The maximum reduction in ductility occurred for the composite containing 6 wt% Al2O3 obtained at 850 rpm. The ductility of the developed composite was reduced by (23 %). The optical microstructures of unreinforced, as-cast Aluminum alloy AA7075 and 6 wt% Al2O3 composites for all stirring speeds show dendrite microstructure resulting from the casting process, but the composite at the stirring speed of 850 rpm shows a more refined microstructure.
Desired mechanical properties like microstructure, micro hardness and wear resistance are the key parameters for which low carbon steel (AISI 1006) are widely selected. Surface heat treatment applied to improve these properties; traditionally surface heat treatments like induction hardening, in recent time’s laser surface hardening. In this work, thermochemical treatment (liquid nitriding) by using mixture from 61% NaCN, 15% K2CO3 and 24% KCL and followed by Nd:YAG laser surface treatment was done . The laser parameter were energy (0.89, 2, 4 and 9) J, spot diameter (0.790 ,0.33, 0.283 and 0.224) mm, pulses duration (1, 2.33, 4.47 and 9.87) ms with fix wavelength 1604nm. Laser surface treatment cycle was melting the layer surface, holding and rapid cooling in air medium. Optical microscopy (OM) and scanning electron microscope (SEM) has been used to study the microstructures and cross-sectional of molted and heat affected zones respectively. The wear test was done to measure the wear rate by using pin -on-disk principles were satisfied. The result shown that increasing in laser energy effects to increase in the area of melted and heat affected zones of nitriding steel. Also increasing in laser energy led to increase micro hardness about 61%, while wear rate decrease about 40 % and increased depth of molted zone.
In this research, we successfully obtained Ni/SiC micro-composite coatings with various contents of SiC particles of particle size(10 ?m), by using electrodeposition method from nickel watts bath in which the SiC particles suspend. The effects of the current density, temperature, and particle loading(PL) of SiC particles in the electrolyte on the morphology, texture, and vol% of SiC in deposit were investigated. The morphological and structural analysis show uniform distribution of SiC particles within the composite coatings. It was found that the depositing conditions affect the microstructure of deposited nickel and the SiC vol% in deposit. Furthermore, the vol% of SiC increases in deposit by increasing the particle loading(PL) in the bath, while decreased by increasing the current density. Also the higher values of SiC vol% were obtained at temperature (50°C).
Friction Stir Welding is one of the most practical welding process at the solid state. Friction Stir Processing is used to enhance the microstructure of FSW welded zone. The present study investigates the effect of welding parameters on the tensile properties of FSW and FSP joining 3 mm AA 5083 - H111 aluminum alloy by means of stress – strain curve with a uniaxial tensile test and by comparing the efficiency between FSW , FSP and base metal .The experiments were conducted with 1000,1500 and 2000 rpm rotation speeds ,and 20,40 and 60 mm/min travel speed. The best result of the welding joint was shown at the 20 mm/min feed speed and 1500 rpm rotational speed for FSW, and 40 mm/min feed speed and 1500 rpm rotation speed for FSP. The efficiency of ultimate tensile strength reaches to 92% for FSW and 94% for FSP.
In the present work the effect of heat treatment processes at different temperatures and in different quenching media on mechanical properties in addition to corrosion behavior in different pH solutions of aluminum alloy 6061 was achieved.The alloy was received as fabricated and the solution heat treatment processes was achieved at temperatures (490,530,570 °C), then quenching for every degree was done in two media (water, oil) to obtain on six samples. The artificial aging was done on every sample at temperature (160°C) for one hour.The microstructure was examined to show Mg2Si in every sample.The results of hardness test showed that the hardness of alloy increased with increasing heat treatment temperatures, and at the same temperature the quenched specimens in oil had higher hardness.On the other hand, the tension tests showed that the strength of alloy increased with increasing of heat treatment temperature, and at the same temperature the quenched specimens in water had higher hardness.The results of corrosions test showed that the heat treatment operations improved corrosion resistance, and the lower value was get upon treating at 530°C.
The corrosion behavior of martensite phase in Cu-Al-Be shape memory alloy with aging at 150 at time 2,4and 6 hour and quenching ice water with salt, water at room temperature and oil media study by open circuit potential, tafal polarization and cyclic polarization. The microstructure of martensite study by optical microscope and x-ray diffraction(XRD) and transformation temperature was determined by Di?erential Scanning Calorimeter (DSC).the result show aging martensite at 150 at 2 and 4 hour have high open circuit potential, low corrosion current density , high corrosion potential and pitting potential than martensite without aging.
Friction stir spot welding (FSSW) is a modern solid-state joining process able to weld similar and dissimilar overlap joints in different classes of materials and is widely being considered for automotive industry. In this work, the mechanical behavior ) i.e. tensile shear tests, Microhardness(, and microstructure of friction stir spot welded joints were studied for AA6061-T6 aluminum alloy sheets with thickness of 1.6 mm. Series of FSSW experiments were conducted using vertical CNC milling machine type "C-tek". FSSW is carried out at different pin profiles (cylindrical, taper, and triangular) and tool rotational typically speeds, i.e. 800, 1000, 1200 and 1400 rpm. Based on the welding experiments conducted in this study, the results show that sheets welded by triangular pin tool have highest tensile shear load, of 3.2 kN, followed by welds with cylindrical pin, while welds made using taper pin has the tensile shear load 2.1 kN at optimum speed of 1200 rpm. Also the pin shape and rotational speed had an obvious effect on microstructural parameters i.e. hook height and bond width.
This research is devoted to study the influence of different weight percent concerning to the additions of Ti and Cu on mechanical and tribological properties of AA6061. The composite materials consist of different weight percentage of Ti (0.2, 0.4, and 0.6) wt% and constant weight percentage of Cu (0.2) wt% which were fabricated by liquid metallurgy route technique. Microstructural characterization and phases have been examined by using SEM (scanning electron microscopic).SEM examination showed uniform distribution of nano Ti and Cu in AA6061. The consequences of mechanical tests demonstrated clear enhancement in mechanical properties, such as ultimate tensile strength, yield strength, young modulus, ductility% and hardness at additive percentage of 0.4% Ti+0.2%Cu nano particles incorporated into molten AA6061. Percentage of enhancement ultimate tensile strength is about 73.3%, yield strength about 82.7%, young modulus is about 21.2%, the Vickers hardness about 42.6% and the decreasing in ductility was about 25.2% compared with the metal matrix (AA6061). The wear rate test was performed by using pin on disc rig for both hybrid nano composite and base metal (AA6061) under various loads (10,15and 20) N with sliding speed (1.282) m/sec at a (10) min’s time. The results showed a decrease in wear rate at 0.4%Ti+0.2%Cu compared with the base metal (AA6061). Improvement percentage of wear rate is about 105% at 20 N load.
Friction stir welding (FSW), a solid-state welding process, it’s involve a welding by friction between two metals or alloys, and also using for the joining of dissimilar materials due to the lower processing temperature over conventional fusion welding, it's include only one pass of welding. Friction Stir Processing (FSP) is a recent outgrowth of the Friction Stir Welding (FSW) process and relies on solid-state deformation to modify the structure of the workpiece, it's involve two pass or more of welding and applied either on the base metal(BM) or to join the two alloys/metals. In this paper the new method used, namely reverse rotation friction stir processing (RFSP), this research aims to study the effect of (RFSP) technique on the mechanical properties of welded alloys. (FSW) includes a single pass of the welding line but the second method (RFSP) involves two pass of welding (forth and back) but the 1st pass with a rotation speed in clockwise and the 2nd pass in counter-clockwise. The alloys used of dissimilar AA 2024 and AA6061 aluminum alloys of (3mm) thickness, the parameters used in this research include different rotational speed (1600, 1800, 2000 and 2200) RPM and one feed speed (25) mm/min. In the tensile test the results of reverse rotation friction stir processing (RFSP) was higher than friction stir welding (FSW) for all rotation speeds of welding except (1800 RPM). In the microhardness measurement the values of hardness for all samples at the nugget zone is higher than the basemetal of 6061-T6 and lower than the basemetal of 2024-T3. The efficiency of ultimate tensile strength reaches to about (72 %) for (RFSP) as compare with value of (FSW) and it’s about (44%) at rotation speed (1600 RPM).The only exception of welding was when the rotational speed of (1800 RPM), where the (FSW) is better than (RFSP), efficiency was approximately (77%) for the (FSW) compared with the results of (71%) (RFSP).
The present work deals with direct diffusion bonding welding without interlayer of austenitic stainless steel type AISI 304L with Oxygen Free High Conductivity pure copper (OFHC) in vacuum atmosphere (1.5 *10-5 mbr.). The optimum bonding conditions are temperature of 650 ?C, duration time of 45 min. and the applied stress of 30 MPa, in order to secure a tight contact between the mating surfaces. The corrosion behavior of diffusion bonding joints in 3.5% Nacl is studied to evaluate the corrosion resistance of welding joints by using Potentiodynamic method. The observed microstructure of corroded specimen of optimum diffusion bonding joint shows that the corrosion current density has low value as compared with base materials used. During polarization, galvanic coupling is observed between two materials used. At passivity region, inverse polarity is occurred at 450mV. Therefore, passive stainless steel 304 L behaves as cathode respective to pure copper, the corrosion behavior of the diffusion bonding joint was mostly by copper side. The corrosion results indicate the presence of galvanic effect. The corrosion current density of copper, stainless steel 304L and bond joints condition were (3.66 µA/cm2, 1.62 µA/cm2 and 1.85µA/cm2) respectively. A SEM examination of corroded diffusion bonding joint indicates that the galvanic corrosion happened on copper side. The corrosion rate of bonding joint conditions was 0.85 mpy, which is less than 1%. This means that corrosion resistance of bond joint is more than excellent.
In this study a Nickel-Titanium-Cupper shape memory alloys was manufactured by powder metallurgy (PM) technique, powder mixture of 50% Ti , 47% Ni and 3% Cu was prepared by mixing for two hours and compacted in a press machine using various compacting pressure (600, 700 and 800) MPa , sample was then sintered for 5 hrs in an electrical tube vacuum furnace using sintering temperature of (850?C, 900?C and 950?C) .phase analysis of samples was conducted by X-ray diffraction test, the effect of different sintering temperature and compacting pressure on the porosity, microhardness ,compression strength and the shape memory effect (SME) was studied, the result showed decrease in the porosity and increasing in the shape recovery ,compression strength and microhardness with increasing compacting pressure and at lower sintering temperature and hence the best results was at 800MPa compacting pressure and 850?C sintering temperature.
This study aims to enhance the compression strength in one type of Pb-Sn-Sb alloys which wellknown by (Babbitt-ASTM B23 Alloy 13). The ?processing doing via equal channel angular extrusion technique. Three casting were implemented to ?manufacture the alloy; Chill Casting (CC), New Rheocasting (NRC) and Gravity Die Casting (GDC). The ?microscope examination shows that the microstructures contain two phases, ?-Pb and cubic shaped ?intermetallic compound (?-SbSn) in a matrix of ternary phases. CC was fine equiaxed as well as NRC, while ?in GDC was a dendrite ?-Pb phase with remaining ?-SbSn phase as a cubic shape. Higher mechanical properties in compression were recorded for Gravity die casting (12.7 %) while the NRC registered the highest value in yield strength (11.7 %). On the other hand, the casting techniques had a slight difference in Young's modulus. The other resulted data like hardness showed that NRC is the first reading (12.55 %) and then gravity casting recorded as second score comparing with other (11.79 %), The results ?showed aslo that increasing forming temperature during angular extrusion has an adverse effect on compression ?strength. The study ?concluded that microstructural change caused by ECAP softens the material due to the break-up the original ? precipitate and accelerate from the dynamic recrystallization.
In this study the friction stir lap welding was carried out by a new technique (diffusion bonding phenomenon) between (AA1100 and low carbon steel C10 sheets of 3mm and 1mm thickness respectively. These alloys have difference ranges in melting temperature and other physical properties. Different parameters were used: tool rotation speeds (630, 1250) rpm, travel speeds (80, 32) mm/min. and pin length (2.8,3) mm using cylindrical threaded pin. Many tests and inspections were performed such as tensile shear test and X-Ray diffraction tests. Microhardness and microstructure observations were conducted by using optical and SEM. The above tests were used to evaluate the weld quality and joint efficiency under different welding parameters. Best result for FSLW by diffusion phenomenon appear in (low carbon steelC10 / AA1100-H112) joint at 1250rpm in 32 mm/min. with 2.8mm pin length and the maximum tensile shear strength was (3.9)KN.It was found that the highest micro hardness was (138HV) at the interface between the low carbon steel and AA1100.